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Setting an experimental measurement around 35pF is on the low side,
where extraneous effects can blur capacitance results.
If desiring to measure k for water, I'd suggest it is better to measure
the effect of a water dielectric. (No extraneous dielectrics...)
I think you will be pleased with results.
As to the high-side anomaly - though I'm not sure this is the cause,
let me ask: what would you expect to read in your setup with a strong
salt solution in the bag? or a thick metal plate in the bag?
Brian Whatcott Altus OK