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Re: [Phys-l] Gas Desorption



Depending on beam energy, electrons and ions can modify the surface somewhat...don't know if that would be a concern. Sulphuric acid tends to leave, as I recall, some adsorbed sulfur which could be a problem.

so, Bernard, are you or were you a surface scientist...what sort of work did you do?

cheers,

joe

Joseph J. Bellina, Jr. Ph.D.
Professor of Physics
Saint Mary's College
Notre Dame, IN 46556

On Nov 25, 2006, at 6:35 PM, Bernard Cleyet wrote:

One may also use electron and ion bombardment and plasma cleaning. In
the case of plasma cleaning it's important to use aluminium electrode(s)
to prevent sputtering.

bc, who once cleaned glass using an ancient method (chromic / sulphuric
acid). Also, substrates w/ electron bombardment and plasma, and just
heat w/ a Varian oilless UHV system.


http://www.faqs.org/faqs/sci/chem-faq/part4/section-1.html


Brian Whatcott wrote:

At 10:23 PM 11/24/2006, Suraj, you wrote:



Suyraj Parkash
38, Azad Nagar, Jagadhri Road,
AMBALA CANTT 133006 (India)
.
NOVEMBER 25, 2006
.
Dear Sirs :
..
I wish to know the procedure to degas and clean
vacuum discharge tubes of gaseous impurities specically in
spectrum analysis gas tubes.

SurajParkash




A vacuum bake-out is a good place to start. 150 to 300 degC
Take a look at the easily accessible literature.
As usual, Google is your friend
<http://www.google.com>

Take a look at this PDF file for example for an example of
extended gas desorption efforts.
(you need an Adobe reader, which is freely accessible.)

<http://pubs.acs.org/cgi-bin/abstract.cgi/ancham/1979/51/i08/f-pdf/ f_ac50044a029.pdf?sessid=6006l3>




Brian Whatcott Altus OK Eureka!


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_______________________________________________
Forum for Physics Educators
Phys-l@carnot.physics.buffalo.edu
https://carnot.physics.buffalo.edu/mailman/listinfo/phys-l