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If you perform electrolysis on a liter of tap water, by time you get
down to 35 mL remaining you theoretically should have nearly pure H-2
H20 (or D2O). It should have a mass substantially greater than 35
grams;
Yes, any chemical reaction is going to preferentially yield
light-isotope products to some degree. However, the effect is only
dramatically substantial in the case of hydrogen.
If that is true, then C-12 CO2 is going to react about 2% (1.02 times)
faster than C-14 CO2.